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1 article(s) from Severin, Tobias

Coordination chemistry and photoswitching of dinuclear macrocyclic cadmium-, nickel-, and zinc complexes containing azobenzene carboxylato co-ligands

Jennifer Klose,
Tobias Severin,
Peter Hahn,
Alexander Jeremies,
Jens Bergmann,
Daniel Fuhrmann,
Jan Griebel,
Bernd Abel and
Berthold Kersting

Beilstein J. Org. Chem. 2019, 15, 840–851, doi:10.3762/bjoc.15.81

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Graphical Abstract

Figure 1: Left: Mixed ligand complexes of the type [M₂L(μ-L')]ⁿ⁺ supported by the macrocyclic ligand H₂L (M =...

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Figure 2: Synthesized compounds and their labels.

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Scheme 1: Synthesis of complexes 1–9.

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Figure 3: ¹H NMR spectrum of 6 in CD₃CN at 295 K (1.0–8.0 ppm). The resonances and assignments are listed in Table 2...

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Figure 4: Structure of the [Zn₂L(μ-azo-OH)]⁺ cation in crystals of [Zn₂L(μ-azo-OH)][Zn₂L(μ-azo-O)]·4MeCN·3H₂O...

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Figure 5: Space filling representation of the packing of two symmetry-related [Zn₂L(μ-azo-NMe₂)]⁺ cations in ...

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Figure 6: Structure of the [Cd₂L(μ-azo-NMe₂)]⁺ cation in crystals of [Cd₂L(μ-azo-NMe₂)]ClO₄·0.5MeOH (6·0.5MeO...

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Figure 7: Space filling representation of the packing of four [Cd₂L(μ-azo-NMe₂)]⁺ cations in crystals of 6·0....

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Figure 8: Structures of the two crystallographically independent [Ni₂L(μ-azo-NMe₂)]⁺ cations A (left) and B (...

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Figure 9: Left: ORTEP representation of the molecular structure of the [Cd₂L(μ-azo-CO₂Me)]⁺ cation in crystal...

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Figure 10: Plots of the effective magnetic moment μ_eff for 2 (open circles), 4 (open squares), and 7 (open tri...

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Figure 11: UV–vis spectra of Hazo-H (red line), [Cd₂L(μ-Cl)](ClO₄) (black line) and [Cd₂L(μ-azo-H)]ClO₄ (1, bl...

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Figure 12: UV–vis spectra of Hazo-NMe₂ (red line), [Ni₂L(μ-Cl)](ClO₄) (black line) and [Ni₂L(μ-azo-NMe₂)]ClO₄ (...

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Figure 13: UV–vis spectra of solutions of [Cd₂L(μ-azo-H)]ClO₄ (1) in acetonitrile irradiated with a UV LED lam...

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Scheme 2: Cis/trans isomerization process of the bound azo-carboxylato co-ligand in [Cd₂L(μ-azo-H)]ClO₄ (1) i...

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Published 03 Apr 2019

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